COURSE UNIT TITLE

: ANORGANIC CHEMISTRY LABORATORY II

DEGREE PROGRAMMES

Description of Individual Course Units

Course Unit Code Course Unit Title Type Of Course D U L ECTS
ELECTIVE

Offered By

Chemistry

Level of Course Unit

First Cycle Programmes (Bachelor's Degree)

Course Coordinator

ASSISTANT PROFESSOR ELIF ANT BURSALI

Offered to

Chemistry
Chemistry (Evening)

Course Objective

The main objective of this course is to synthesize and purify coordination compounds, characterize them with different methods and to interpret the results of the experiments.

Learning Outcomes of the Course Unit

1   Synthesize hexaammincobalt(III) chloride and chloropentaaminecobalt(III) chloride.
2   Synthesize potassium trioxalatochromate(III) trihydrate.
3   Synthesize tetraaminecuprate(II) sulfate monohydrate and hexaaminenickel(II) chloride
4   Determine properties of complexes using crystal field theory and electronic spectroscopy.
5   Synthesize nitritopentaaminecobalt(III) chloride and nitropentaaminecobalt(III) chloride
6   Differentiate nitro and nitrito binding isomers by IR spectroscopy .
7   Associate conductometric determination of conductivity in coordination compounds with Werner theory.
8   Synthesize trans-bis (ethylenediamine) dichlorocobalt (III) chloride and discuss acid hydrolysis kinetics of trans-[Co(en)2Cl2]+ complex ion.

Mode of Delivery

Face -to- Face

Prerequisites and Co-requisites

None

Recomended Optional Programme Components

None

Course Contents

Week Subject Description
1 Inorganic Chemistry Laboratory-II Introduction and Preparation
2 Synthesis of hexaammincobalt(III) chloride
3 Synthesis of chloropentaaminecobalt(III) chloride
4 Synthesis of potassium trioxalatochromate(III) trihydrate
5 Synthesis of tetraaminecuprate(II) sulfate monohydrate
6 Synthesis of hexaaminenickel(II) chloride
7 Investigation of the Properties of Complexes Using Crystal Field Theory and Electronic Spectroscopy
8 Mid-term
9 Synthesis of nitritopentaaminecobalt(III) chloride and nitropentaaminecobalt(III) chloride
10 IR spectroscopy for Binding Isomers
11 Werner Theory and Conductometry
12 Synthesis of trans-bis (ethylenediamine) dichlorocobalt (III) chloride
13 Acid hydrolysis kinetics of trans-[Co(en)2Cl2]+ complex ion.
14 Make up Experiments

Recomended or Required Reading

Huheey, J.E. (1972). Inorganic Chemistry, Harper International Edition, Newyork.
Shriver, D. F., Atkins, P. W., Langford, C. H. (1994). Inorganic Chemistry, Oxford University Press, Oxford.
Woollins, J. D. (2010) Inorganic Experiments, Third Edition, Wiley-VCH, Weinheim.
Svehla, G. (1996) Vogel s Qualitative Inorganic Analysis, Longman, U.K.

Planned Learning Activities and Teaching Methods

Application, Homework, Quiz

Assessment Methods

SORTING NUMBER SHORT CODE LONG CODE FORMULA
1 MTE MIDTERM EXAM
2 QUZ QUIZ
3 ASG ASSIGNMENT
4 FIN FINAL EXAM
5 FCGR FINAL COURSE GRADE (RESIT) MTE* 0.30 + QUZ * 0.20 + ASG * 0.10 + FIN * 0.40
6 RST RESIT
7 FCGR FINAL COURSE GRADE (RESIT) MTE * 0.30 + QUZ * 0.20 + ASG * 0.10 + RST * 0.40


*** Resit Exam is Not Administered in Institutions Where Resit is not Applicable.

Further Notes About Assessment Methods

None

Assessment Criteria

The student is evaluated by taking into consideration of quiz, average grade of reports prepared after the experiments (homework)and the questions asked in the midterm and final exams.

Language of Instruction

Turkish

Course Policies and Rules

Attendance to at least 80% for the lectures is an essential requirement of this course and is the responsibility of the student. It is necessary that attendance to the lecture and homework delivery must be on time. Any unethical behavior that occurs either in presentations or in exams will be dealt with as outlined in school policy. You can find the undergraduate policy at http://web.deu.edu.tr/fen

Contact Details for the Lecturer(s)

Dokuz Eylul University, Faculty of Science, Chemistry Department e-mail: m.yurdakoc@deu.edu.tr, elif.subasi@deu.edu.tr, senem.karahan@deu.edu.tr, elif.ant@deu.edu.tr

Office Hours

Thursday 15:00-17:00

Work Placement(s)

None

Workload Calculation

Activities Number Time (hours) Total Work Load (hours)
Tutorials 13 3 39
Preparations before/after weekly lectures 12 1 12
Preparation for midterm exam 1 3 3
Preparation for final exam 1 4 4
Preparing assignments 12 1 12
Final 1 2 2
Midterm 1 2 2
Quiz etc. 1 1 1
TOTAL WORKLOAD (hours) 75

Contribution of Learning Outcomes to Programme Outcomes

PO/LOPO.1PO.2PO.3PO.4PO.5PO.6PO.7PO.8PO.9PO.10PO.11PO.12PO.13PO.14PO.15PO.16PO.17
LO.15555
LO.25555
LO.35555
LO.45555
LO.55555
LO.655525
LO.75555
LO.8555435

CONTACT INFORMATION
Dokuz Eylül Üniversitesi Cumhuriyet Bulvarı No: 144 35210 Alsancak / İZMİR
Phone: +90(232) 412 12 12 - Fax: +90 (232) 464 81 35

Copyright 2015 DEÜ. BİD

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