COURSE UNIT TITLE

: SPECTROSCOPIC METHODS AT STRUCTURAL ANALYSIS OF ORGANIC COMPOUNDS

DEGREE PROGRAMMES

Description of Individual Course Units

Course Unit Code Course Unit Title Type Of Course D U L ECTS
KIM 5069 SPECTROSCOPIC METHODS AT STRUCTURAL ANALYSIS OF ORGANIC COMPOUNDS ELECTIVE 3 0 0 8

Offered By

Graduate School of Natural and Applied Sciences

Level of Course Unit

Second Cycle Programmes (Master's Degree)

Course Coordinator

ASSOCIATE PROFESSOR GÜLSIYE ÖZTÜRK ÜRÜT

Offered to

Chemistry
Chemistry

Course Objective

The aim of this course is to provide students to understand the theory of spectroscopic techniques (UV, IR, 1H-NMR, 13C-NMR, MS) and interpretation of spectra and apply these knowledge in interpreting the structure of unknown molecules

Learning Outcomes of the Course Unit

1   Discuss which information can be obtained from spectroscopic techniques used in structural identification of organic compounds
2   Comment about the conjugation level of organic compounds by using UV-Vis absorption and fluorescence spectroscopy methods
3   Interpret the mass spectra of organic compounds
4   Determine the functional groups of organic compounds by FT-IR spectroscopy
5   Learn what kind of information can be get by interpreting the 1H NMR and 13C NMR spectra of organic compounds

Mode of Delivery

Face -to- Face

Prerequisites and Co-requisites

None

Recomended Optional Programme Components

None

Course Contents

Week Subject Description
1 Introduction to spectroscopic methods
2 UV-Vis spectroscopy and applications
3 Fluorescence spectroscopy and applications
4 Introduction to IR Spectroscopy, Functional Group Frequencies of Organic Compounds, Factors Affecting IR vibrational frequencies
5 Types of mass spectrum peak, Determination of Molecular Formula, molecular fragmantation
6 Introduction to 1H-NMR spectroscopy, structure determination with 1H-NMR, chemical shift
7 Introduction to 13-CNMR spectroscopy, structure determination with13-CNMR, chemical shifts
8 The evaluation of UV, IR, mass and NMR spectra together
9 Homework
10 Homework
11 Homework
12 Analysis of Organic Compounds Integrated Spectrum
13 Analysis of Organic Compounds Integrated Spectrum
14 Spectra Analysis Applications

Recomended or Required Reading

R.M. Silvertein, F.X. Webster, Spectrometric Identification of Organic Compounds, USA: John Wiley & Sons Inc. ,1998
D. L. Pavia, G. M. Lampman, G. S. Kriz, Introduction to Spectroscopy: A guide for students of organic chemistry, Saunders College Publishing, 1979
Ender Erdik, Organik Kimyada Spektroskopik Yöntemler, Gazi Kitabevi, 2005

Planned Learning Activities and Teaching Methods

Pressentation, describing the subject, question-answer, sampling, homework

Assessment Methods

SORTING NUMBER SHORT CODE LONG CODE FORMULA
1 ASG ASSIGNMENT
2 FIN FINAL EXAM
3 FCG FINAL COURSE GRADE ASG * 0.50 + FIN * 0.50
4 RST RESIT
5 FCGR FINAL COURSE GRADE (RESIT) ASG * 0.50 + RST * 0.50


Further Notes About Assessment Methods

None

Assessment Criteria

Student will be assessed with homework presentation and questions which will be asked in final exam

Language of Instruction

English

Course Policies and Rules

During the semester, the responsibility to continues 70% of the courses is student s self-owned. And must be observed the specified time about course times. Unethical behavior that may occur in class and on exams, will be acting within the framework of the relevant regulations. Teaching and examination implementation principles regulations of D.E.Ü Graduate School of Natural and Applied Sciences can be found at Graduate School of Natural and Applied Sciences web page.

Contact Details for the Lecturer(s)

Dokuz Eylul University, Faculty of Science, Department of Chemistry e-mail: gulsiye.ozturk@deu.edu.tr

Office Hours

Wednesday, Thursday 15.00-17.00

Work Placement(s)

None

Workload Calculation

Activities Number Time (hours) Total Work Load (hours)
Lectures 10 3 30
Preparations before/after weekly lectures 10 3 30
Preparation for final exam 1 75 75
Preparing assignments 3 20 60
Final 1 4 4
TOTAL WORKLOAD (hours) 199

Contribution of Learning Outcomes to Programme Outcomes

PO/LOPO.1PO.2PO.3PO.4PO.5PO.6PO.7PO.8PO.9PO.10PO.11
LO.133222232
LO.233222232
LO.333222232
LO.433222232
LO.533222232

CONTACT INFORMATION
Dokuz Eylül Üniversitesi Cumhuriyet Bulvarı No: 144 35210 Alsancak / İZMİR
Phone: +90(232) 412 12 12 - Fax: +90 (232) 464 81 35

Copyright 2015 DEÜ. BİD

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