COURSE UNIT TITLE

: CONVENTIONAL AND TANDEM MASS SPECTROMETRY TECHNIQUES AND APPLICATIONS

DEGREE PROGRAMMES

Description of Individual Course Units

Course Unit Code Course Unit Title Type Of Course D U L ECTS
KIM 5076 CONVENTIONAL AND TANDEM MASS SPECTROMETRY TECHNIQUES AND APPLICATIONS ELECTIVE 3 0 0 7

Offered By

Graduate School of Natural and Applied Sciences

Level of Course Unit

Second Cycle Programmes (Master's Degree)

Course Coordinator

PROFESSOR KADRIYE ERTEKIN

Offered to

Chemistry
Chemistry

Course Objective

The course aims to provide an introduction to mass spectrometry techniques, to give a detailed presentation of mass spectrometry especially in terms of instrumentation and its applications in chemical analysis. Instrumentation, ion source technologies, mass analyzer technologies, magnetic sector time-of-flight, quadruple, Fourier transform ion cyclotron resonance analyzers and detector systems will be given. Tandem mass spectrometry techniques will be given into detail. GC-MS, LC-MS, MS-MS and ICP-MS techniques are the subjects of this course.

Learning Outcomes of the Course Unit

1   This course is expected to help the students to provide an introduction to mass spectrometry techniques into detail in terms of instrumentation and theory, to make an assessment on analysis with mass spectroscopy
2   To develop the students analytical abilities and ability to criticize and solve problems regarding instrumental analysis with MS.
3   To give the students further information on tandem MS techniques.
4   Students are expected to know the analytical approaches exploiting MS techniques.
5   Students are expected to know and make assessment advantages and disadvantages of the existing MS techniques over each other.

Mode of Delivery

Face -to- Face

Prerequisites and Co-requisites

None

Recomended Optional Programme Components

None

Course Contents

Week Subject Description
1 An introduction to mass spectrometry techniques, history, and development
2 Instrumentation, magnetic sector analysers, time-offlight analysers.
3 Instrumentation, quadrupole, fourier transform ion cyclotron resonance analysers
4 Instrumentation:detector systems will be given
5 Instrumentation: , ion source Technologies, ionization techniquies
6 Instrumentation: general assessment regarding instrumentation
7 Choise of instrument considering the sample
8 Tandem mass spectroscopy techniques (MS-MS)
9 ICP_MS
10 ICP MS and its applications in analysis
11 MALDI MS technique (Presentation of students)
12 Gas Chromatography- Mass Spec. GC-MS ad choice of analyte (Presentation of students)
13 Liquid Chromatography- Mass Spec. LC-MS ad choice of analyte (Presentation of student projects)
14 Presentation of student projects

Recomended or Required Reading

1. Sparkman, O. David (2000). Mass spectrometry desk reference. Pittsburgh: Global View Pub. ISBN 0-9660813-2-3.
2. Principles of Instrumental Analysis Douglas A. Skoog, F. James Holler and Timothy A. Nieman Harcourt Brace College Publishers
3. Mass Spectrometry: Principles and Applications (2nd ed.), Edmond de Hoffman; Vincent Stroobant (2001). John Wiley and Sons. ISBN 0-471-48566-7.
4. Price, Phil (1991). "Standard definitions of terms relating to mass spectrometry. A report from the Committee on Measurements and Standards of the American Society for Mass Spectrometry". Journal of the American Society for Mass Spectrometry 2 (4): 336 348. doi:10.1016/1044-0305(91)80025-3

Planned Learning Activities and Teaching Methods

Lecture, presentation, project based learning

Assessment Methods

SORTING NUMBER SHORT CODE LONG CODE FORMULA
1 MTE MIDTERM EXAM
2 ASG ASSIGNMENT
3 FIN FINAL EXAM
4 FCG FINAL COURSE GRADE MTE * 0.20 + ASG * 0.20 + FIN * 0.60
5 RST RESIT
6 FCGR FINAL COURSE GRADE (RESIT) MTE * 0.20 + ASG * 0.20 + RST * 0.60


Further Notes About Assessment Methods

None

Assessment Criteria

To be announced.

Language of Instruction

English

Course Policies and Rules

Has been shown in DEBIS menu

Contact Details for the Lecturer(s)

DEU Faculty of Science Department of Chemistry
e-mail: kadriye.ertekin@deu.edu.tr
Tel: 0 232 3018691

Office Hours

To be announced.

Work Placement(s)

None

Workload Calculation

Activities Number Time (hours) Total Work Load (hours)
Lectures 12 3 36
Presentations by students 4 3 12
Preparation before/after weekly lectures 12 5 60
Preperations for final exam 1 30 30
Preparing Individual Assignments 12 2 24
Final 1 3 3
TOTAL WORKLOAD (hours) 165

Contribution of Learning Outcomes to Programme Outcomes

PO/LOPO.1PO.2PO.3PO.4PO.5PO.6PO.7PO.8PO.9PO.10PO.11
LO.1555555
LO.2555555
LO.354555
LO.4555555
LO.555555

CONTACT INFORMATION
Dokuz Eylül Üniversitesi Cumhuriyet Bulvarı No: 144 35210 Alsancak / İZMİR
Phone: +90(232) 412 12 12 - Fax: +90 (232) 464 81 35

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